GC9890+HS16A dedicated chromatograph for detecting 21 VOCs in tobacco packaging ink
Sales phone number:/ fifty-seven million seven hundred and eighty-six thousand three hundred and eleven
Technical Department: 13761342293
Instrument analysis scope
Detect trace amounts of volatile organic compounds (VOCs) such as benzene, toluene, ethylbenzene, xylene (ortho, meta, para), ethanol, isopropanol, n-butanol, acetone, 4-methyl-2-pentanone, butanone, cyclohexanone, ethyl acetate, n-propyl acetate, n-butyl acetate, isopropyl acetate, and propylene glycol methyl ether in cigarette strips, packaging paper, and printing ink. The detection limit for benzene is ≤ 0.002mg/m2
Analysis principle (fully compliant with tobacco industry standards YC/T207-2006 and YC263-2008)
In a closed container and at a certain temperature, volatile components in the sample exist in equilibrium between the gas phase (headspace) and the matrix (liquid or solid phase). When reaching equilibrium, the gas phase is introduced into the gas chromatography for separation. After matrix calibration, the content of each volatile component in the sample can be determined, which is the headspace gas chromatography (HS-GC) method
Analysis conditions:
Chromatograph: GC-9890B headspace gas chromatograph; Capillary chromatography column: 60m imported column from the United States
Injector temperature: 150 ℃ Detector temperature: 250 ℃ Pre column pressure 0.06Mpa
Column box temperature: Hold at 40 degrees for 2 minutes, increase to 180 degrees per minute at 4 degrees, and hold for 15 minutes.
Standard sample chromatogram:
Table 1: Standard curves and linear correlation coefficients of five level concentration standards for seven benzene derivatives, including benzene
component | Standard Curve | Linear correlation coefficient |
benzene | Y=7.8937×10-6X* | 0.999987 |
toluene | Y=1.80059×10-5X | 0.999999 |
ethylbenzene | Y=2.08552×10-5X | 0.999993 |
P-Xylene | Y=2.06973×10-5X | 0.999993 |
xylene | Y=1.98165×10-5X | 0.999976 |
O-Xylene | Y=2.42661×10-5X | 0.999986 |
STYRENE | Y=3.17404×10-5X | 0.999989 |
*X is peak area, y is component concentration (mg/m)2)
Update time: August 10, 2020 17:18:32