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Feed atomic absorption spectrometer
The use of feed atomic absorption spectrometer products in feed analysis: to detect the content of trace metal elements such as copper, iron, zinc, ma
Product details

Implementation standard for feed atomic absorption spectrometer: Announcement No. 1849 of the Ministry of Agriculture, "License Conditions for Feed Production Enterprises" and "License Conditions for Mixed Feed Additive Production Enterprises", announced by the Ministry of Agriculture on October 22, 2012, and implemented from December 1, 2012

Trace elements that can be detected: copper, iron, zinc, cobalt, manganese, lead, cadmium, chromium, etc. (arsenic and mercury content are generally not measured, if necessary, accessories such as hydride generators should be added)

Application case of atomic absorption spectrophotometer: detectable items of the instrument: metal elements and trace heavy metal elements

y=0.0838x+0.0024 r=0.9995

The specific instrument performance parameters are introduced as follows: computer-controlled single flame atomic absorption spectrophotometer: a precision instrument mainly used to detect the content of trace metal elements in various substances. It can detect more than 40 elements including manganese, iron, copper, zinc, lithium, sodium, magnesium, iron, potassium, calcium, chromium, cobalt, nickel, arsenic, selenium, silver, cadmium, indium, tin, antimony, platinum, gold, lead, etc. It is mainly detected by flame method, and the detection limit can generally be PPM level (parts per million content)

1、 Performance indicators of feed atomic absorption spectrometer

1. Optical system
Automatic adjustment of wavelength range 190nm-900nm
Grating engraved line density 1800 lines
Monochromator aberration correction Czerny Turner type monochromator
Spectral bandwidth of 0.1, 0.2, 0.4, 1.0, and 2.0nm, with multiple automatic switching modes
Wavelength accuracy ± 0.20nm
Wavelength repeatability of 0.1nm
Baseline drift static 0.005A/30min dynamic 0.008A/30min
Detector wide spectral range photomultiplier tube
The resolution can distinguish the dual lines of 279.5nm and 279.8nm in the manganese lamp, and the energy of the valley between the two spectral lines should be less than 20%

2. Light source system
Lamp holder 3 lamp holder
Lamp power supply method: 400Hz square wave pulse
Lamp current regulation range 0-10mA average current
3. Atomization system
Flame analysis method
Detection limit (Cu) 0.006 μ g/ml
Burner 100mm all titanium metal burner
Precision RSD ≤ 1%
Spray metal sheathed high-efficiency glass spray
Corrosion resistant all plastic atomization chamber
The safety measures have multiple automatic safety protection functions, including acetylene leakage alarm and automatic shutdown system
Flameless (graphite furnace) analysis method
Detection limit (Cd) ≤ 4pg

4. Flame analysis method and measurement method

Air acetylene flame method, hydride generator atomic absorption method
The concentration calculation method automatically fits the working curve, automatically corrects sensitivity, and calculates concentration and content.
Repeat measurements 1 to 99 times, automatically calculate the mean, content, standard deviation, and relative standard deviation.
Print test data or final analysis report as a result. The results can be exported as an Excel worksheet.
Software environment: Windows XP/Vista operating system, professional Chinese software

2、 Parameters

Power supply AC 220V/50HZ
Power 150VA
Net weight of the instrument 55kg
Instrument gross weight 80kg
Instrument volume 1110mm (horizontal) x 400mm (depth) x 500mm (height)
Packaging volume 1350mm (horizontal) x 600mm (depth) x 850mm (height)
Working environment temperature: 10-35 ℃
Working environment humidity ≤ 80%

3、 Standard configuration
1. Host
2. Low noise oil-free air compressor
3. Three hollow cathode lamps
4. Operating software

4、 Design Features

1. Total reflection optical system with chromatic aberration reduction across the entire wavelength range. After adjusting the focal point, any wavelength can be changed, and the focal point will no longer change. The wavelength will be automatically scanned and peak searched.

2. It has a deuterium lamp buckle background and a self-priming buckle background.

3. The uniquely designed all titanium burner ensures smooth combustion and fast thermal equilibrium speed.

4. Automatically adjust negative high voltage, lamp current, and element lamp position to maximize energy, and provide automatic gas leakage and flameout protection. 3 hollow cathode lamp stands. Automatic control system, capable of automatically scanning wavelengths. Preheat one element lamp and preheat the other two element lamps.

5. Graphite furnace heating: Users can freely set the heating curve according to their needs.

Sensitivity and detection limit of commonly tested elements in the feed industry

element

Wavelength (nm)

Flame method

Sensitivity (ug/ml ppm)

Detection limit (ug/ml ppm)

Cu

324.75

0.025

0.006

Fe

248.30

0.05

0.003

Mn

279.48

0.03

0.003

Zn

213.85

0.007

0.0026

Pb

283.30

0.1

0.01

Ni

232.00

0.037

0.007

Bi

306.7

0.22

0.07

Ca

422.67

0.01

0.002

Cd

228.88

0.015

0.005

Cr

357.90

0.04

0.003

Cs

455.5

0.058

0.019

K

766.49

0.02

0.003

Li

670.78

0.023

0.0016

Mg

285.21

0.0037

0.0002, , , ,

Mo

311.20

0.28

0.046

Na

588.99

0.005

0.00023

Pt

271.9

1.0

0.098

Sb

231.2

0.28

0.06

Sc

327.4

0.25

0.03

Se

204.0

0.11

0.016

Sn

266.1

0.88

0.16

Sr

460.73

0.06

0.001

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